Hanyar samar da gargajiya na inositol shine matsa lamba hydrolysis. Saboda shekaru na ?warewar samar da masana'antu, hanyar hydrolysis matsin lamba shine babban fasahar tsari da masana'antun gida suka kar?a kuma an ci gaba da ha?akawa a cikin samarwa. A general tsari na matsa lamba hydrolysis Hanyar ne kamar haka: phytin (hydrolysis) → hydrolysis bayani (neutralization, tacewa) → inositol bayani (najasa kau da maida hankali, crystallization centrifugation) → danyen inositol (rushe da ?azanta kau, crystallization centrifugation) → lafiya samfurin. Daga cikin su, hydrolysis da refining sune matakai biyu masu mahimmanci.
Sodium phytate hydrolysis
Yin amfani da ruwan masara da aka ji?a a matsayin ?anyen abu, ana samar da sodium phytate ta hanyar ion musayar resin adsorption, sa'an nan kuma an fuskanci matsin lamba na hydrolysis don samar da inositol. A daidai lokacin da ake samar da inositol, ha?in gwiwar samar da disodium hydrogen phosphate (samar da disodium hydrogen phosphate ya kai ninki 12 na inositol) yadda ya kamata ya dawo da sinadarin phosphorus daga hatsi, yana bu?e wata sabuwar hanya don dawo da sinadarin phosphorus a cikin kayayyakin noma da na gefe.
Bayanin tsari na samarwa: Ana shayar da ruwan masara ta hanyar ion musayar guduro don samun wani nau'i na maganin sodium phytate, wanda ke fuskantar matsin lamba na hydrolysis don samar da inositol da disodium hydrogen phosphate. Bayan wani lokacin dauki, ana fitar da kayan, tacewa, sanyaya, da crystallized, wanda ya haifar da hazo na disodium hydrogen phosphate crystals. Maganin amsawar hydrolysis na sodium dihydrogen phosphate lu'ulu'u ana sabunta su ta hanyar anion da resin musanya cation har sai adadin anions da cations a cikin maganin amsawar hydrolysis ya kai ?ayyadaddun ma'auni. The mai ladabi hydrolysis dauki bayani za a iya mayar da hankali da kuma crystallized don samun ??re samfurin inositol. Abubuwan da ake samu na inositol sun fi shafar abubuwa uku: lokacin amsawar hydrolysis, matsin lamba na hydrolysis, da tattarawar maganin sodium phytate. Ta hanyar gwaje-gwajen orthogonal, an sami mafi kyawun yanayin halayen halayen hydrolysis kamar haka: lokacin hydrolysis na sa'o'i 7-8, maida hankali na sodium phytate na 20%, matsin lamba na hydrolysis na 1.5 MPa, da matsakaicin yawan amfanin ?asa na inositol daga 0.1544% zuwa 0.1722%. Don lura da tasirin ha?akawa na reactor na hydrolysis, toshewar gado a hasumiya na ion musayar masana'antu, canje-canje a cikin ?arfin musanya, da kwaikwaya manyan yanayin aiki na wurare dabam dabam da aka yi amfani da su a cikin matakin farfadowa na kayan aikin masana'antu, an gudanar da gwajin matukin jirgi akan na'urar da ke da ?arfin sarrafawa na 600m / a ?ar?ashin yanayin halayen da ke sama. Matsakaicin yawan amfanin ?asa na inositol shine 0.1601% (fiye da sau 2.5 sama da hanyar calcium phytate, kuma ingancin samfurin ya dace da alamomi daban-daban da aka ?ayyade a cikin National Pharmacopoeia), wanda ya yi daidai da ?ananan bayanan gwajin.
Hanyar yanayin matsa lamba
Hanyar matsi na yanayi wata sabuwar hanya ce ta samar da inositol da aka saba ha?aka kuma aka sanya shi cikin masana'antu a kasar Sin a cikin 'yan shekarun nan. Its hydrolysis da tace suna da musamman halaye. Mahimman fasali:
(1) Mahimmanci yana rage zuba jari na lokaci ?aya a cikin kayan aiki, kuma zai iya adana fiye da 50% na zuba jari na kayan aiki lokacin da sikelin ya kasance;
(2) Yin amfani da phytin hydrolysis mai kara kuzari yana raguwa da sake zagayowar samarwa kuma yana inganta ?imar amfani da albarkatun ?asa;
(3) An inganta tsarin tsaftacewa, yana haifar da karuwa a cikin ingancin samfurin da yawan amfanin ?asa.
Tsarin catalytic matsa lamba na yanayi: Wani kaso na mai kara kuzari (wanda ya ?unshi glycerol, urea, da calcium carbonate) ana ?ara zuwa wani yanki na maganin phytin a matsa lamba na yanayi, kuma mai zafi don hydrolysis. Bayan hydrolysis, tacewa, crystallization, bushewa, da sauran matakai, inositol za a iya samu. Saboda halayen halayen mai kara kuzari, inositol za a iya yin crystallized a cikin tafi ?aya, yana haifar da mafi kyawun samfuran ??re da sau?a?e tsarin. Ana iya sake yin amfani da abubuwan kara kuzari.